citric acid specification pdf
117 guilliermondii and Candida lipolytica as allowed organisms for production of citric acid through microbial 118 fermentation. download 1 file . GENERAL INFORMATION Article number: 2.01501.112 Product denomination: Citric acid solution Product description: Seasoning for fine bakerys, cremes, jellys and ice cream 2. Accumulation is not expected 12.5 Results of PBT and vPvB assessment . PRODUCT SPECIFICATION Rev. Specific treatments are however also specified. Melting point (C) 153C Relative density 1.542g/cm3 @ 20C Bulk Density 900 kg/m3 pH-Value, Diluted Solution 1.6 @ 100g/l Solubility . Title: Microsoft Word - Citric Acid Anhydrous Spec TCC.docx Author: Sam Bari Created Date: 9/18/2012 8:24:10 AM - The compound is soluble in water (65 - 69.9% w/w +10, +20 and +30C) and Citric acid (H 4 Cit) is an essential component of the Krebs cycle and a universal intermediate in plant and animal metabolism. [21] The speciation diagram shows that solutions of citric acid are buffer solutions between about pH 2 and pH 8. If you need to meet the industry specifications of ASTM A380, A967, B600, F983 or F86, CitriSurf is the recommended citric acid solution for stainless steel and other alloys. They can quantitatively determine the amount of juice by measuring the amount of citric acid. Citric acid 77-92-980 - 100% Citric acid Notes: The actual percentage concentration has been withheld as a trade secret. Citric Acid, Anhydrous Safety Data Sheet according to Federal Register / Vol. It is anhydrous or . Inhalation . Procedure for Pickle (Citric Acid Method) for Carbon Steel: Pickle in a solution of 3-1/2 gal of water per lb of citric acid (required anhydrous granular citric acid). Essentially, the cycle involves converting the potential energy of a variety of nutrients into the readily available energy of adenosine triphosphate (ATP). The procedure commonly used to do this takes advantage of the PDF download. Polyvinylidene Flouride (PVDF) is a strong, tough, abrasion-resistant fluoroplastic material. Stage 6 Harmonization 2 Citric Official August 1, 2012 Change to read: Standard solution C: Dilute 0.75 mL of Standard stock solution C with dilute hydrochloric acid (10g/L) to 100 CLARITY OF SOLUTION mL. Name : Citric Acid, anhydrous, ACS Grade IUPAC name 2-Hydroxypropane-1,2,3-tricarboxylic acid Cat. Armour Specialty Marketing 2080 N Hwy 360, Suite 200 Grand Prairie, Texas 75050 Telephone (972) 660-9980 Fax (972) 660-3176 PRODUCT: LARD PRODUCT NUMBER: 50560 (1/50 lb.) These tests include the following practices: 1.4.1 Practice A Water Immersion Test, 1.4.2 Practice B High Humidity Test, 1.4.3 Practice C Salt Spray Test, It is mainly used as an acidifier, flavoring and chelating agent. Citric acid is a naturally occurring acid which, as implied in the name, is found in all citrus fruits. FIRST-AID MEASURES . Its biocompatibility, hydrophilicity and general safety make. 12 (mcg) 0 0 0 0 0 . 1.1 Commercial product name: Citric Acid Anhydrous 1.2 Chemical characterisation: Organic acid - 2-hydroxy 1,2,3-propanetricarboxylic acid 1.3 Formula: C6H8O7 1.4 Molecular weight: 192.13 1.5 CAS No: 77-92-9 1.6 EINECS No: 201-069-1 1.7 FOR USE IN FOOD (E330) 1.8 Manufactured by: Archer Daniels Midland Company, East Moore St. Rinse with plenty of water for at least 15 minutes and seek medical attention if necessary. Citric acid is a white or colourless crystalline powder and has a low vapour pressure: 1.6 E-10 Pa at +25C (O'Conner, B, 2006). Properties: Let us look into the properties of citric acid in the table below. Citric acid, ACS reagent, 99.5% C0759 Citric acid, 99% 791725 Citric acid, anhydrous, free-flowing, Redi-Dri, ACS reagent, 99.5% 27109 Citric acid, meets analytical specification of Ph. CAS 77-92-9, chemical formula (HOOCCH)C(OH)COOH. Don't get me wrong, some of the "old" . Method 2- Passivation in Citric Acid (4-10w% Citric Acid, various temperature/time ratios are offered and additional wetting agents and inhibitors are acceptable) The following types may be specified for Method 1: Type 1 - Low temperature nitric acid with sodium dichromate (20-25v% nitric, 2-3w% sodium dichromate, 70-90F, 30 mins min) Packaging: 25kg net composite paper-plastic bags or 3-ply kraft paper bags with PE liner, 500kg or 1000kg net PP woven Jumbo bags. Heat and maintain pickling solution between 82 and 88 C (180 and 190 F). Based on our 15 years in food additives & ingredients market, we have a knowledge of China market and manufacturers. produced significant amounts of citric acid. Very good sequestering abilities round off the properties of these products and qualify them for numerous other applications in areas like pharmaceuticals . Citric 5: Other combinations of temperature time and concentration of citric acid with or without chemicals to enhance cleaning, accelerants or inhibitors capable of producing parts that pass the . Introduction. Therefore, volatilisation is not expected to significantly contribute to the dissipation of citric acid in the environment. Title; It has a role as a food acidity regulator, a chelator, an antimicrobial agent and a fundamental metabolite. Eur., BP, ChP, JP, USP 77, No. Specifications Analytical Details Specifications Color Red:3.5 Max Free Fatty Acids as Oleic:0.1% Max Peroxide Value:1 meq/kg Max Specific Gravity:0.920-0.925 Flash Point:> 625 when FFA < 0.05% Mettler Dropping Point:155 Additives:Citric Acid (as preservative) Antioxidants:None Anti-Foaming Agents:None Date: 06/01/2010 Citric acid anhydrous for synthesis. 192.12g/mol Water Balance 7732-18-5 231-791-2 H. 2. Citric acid 99.5 to 100.5 201-069-1 77-92-9 . Glycolic and sulfamic products may be combined in the well. - Find MSDS or SDS, a COA, data sheets and more information. Optimization of Citric Acid Passivation Solution - ASTM A 967 allows solutions containing 4 to 10 weight % citric acid at solution temperatures ranging from 70 to 160 oF. This acid is usually found in citrus fruits like lemons, oranges etc. which are the best examples of having citric acid as the principal constituent. specifications. : AC423560000; AC423560020; AC423560050; AC423560100; AC423565000 CAS No 77-92-9 Synonyms 2-Hydroxy-1,2,3-propanetricarboxylic acid Recommended Use Laboratory chemicals. Citric acid has also been used in preparations for the treatment of gastrointestinal disturbances and chronic metabolic acidosis caused by chronic renal insufficiency or syndrome of renal tubular acidosis [1,2,4-6,20,21,79]. O 18.00 g/mol . Number : 67341A, 500g 67341B, 1kg 67341C, 2,5kg CAS: 77-92-9 EC Number 201-069-1 Structure: C6H8O7 Molecular Weight : 192.13 Storage: Room temperature (Z) Keep dry Specifications Citric Acid, anhydrous 168789 Test Specification Any recommendations or suggestions are made without guarantee or representation as to results and are subject to change without notice. Citric Acid is mainly used as acidulant, flavoring agent, preservative and antistaling agent in food and beverage industry. Protective gloves must satisfy the specifications of EU . 16 (2014), superseding specifications prepared at the 53rd JECFA (1999), published in FNP 52 Add 7 (1999). citric acid (5.5 percent) solution that is injected into a diluted water stream of peroxyacetic acid (PAA) [100 PPM or less], hydrogen peroxide , acetic acid, and 1-hydroxyethylidine-1,1-diphosphonic acid (HEDP) (FCN 993) - to lower the pH of the PAA water stream from Citribel is the only genuinely circular producer of citric acid, citrates, and other high-value co-products through natural surface fermentation of sugar molasses. Citric Acid Anhydrous, USP/FCC (Excipient/Food Use) 020410, 020420, 020440 Acidulant Archer Daniels Midland Co. Technical Services Phone: 217-451-7418 Fax: 217-451-2473 The information contained herein is correct as of the date of this document to the best of our knowledge. Careful solution control, including water purity, ppm (parts per SYNONYMS INS No. Pump the solution through the pipe or immerse pipe in a pickling tank until clean. Weifang ensign industry co. ltd offers a wide range of products which includes Citric acid monohydrate. 441.3.2 If citric acid is used, it shall be added to and incorporated into the liquid whole eggs 1.4 The tests in this specification are intended to confirm the effectiveness of passivation, particularly with regard to the removal of free iron and other exogenous matter. Fluoroplastics (PVDF, HALAR, PTFE, FEP, PFA) Pipe Materials. As expected, another compound identified in the grumixama pulp was citric acid (m/z = 191), since this is a natural source of organic acid, found in all citrus fruits (Aghera & Bhatt, 2019),. Citric acid C 3 H 4 (OH)(COOH) 3 1% 20 0 0 1% K 0 0 5% 20-50 0 0 5% 85-K 0 0 5% 140 1 0 10% 20-40 0 0 10% 85-K 0 0 25% 20 0 0 25% 40 0 0 25% 85 1 0 continued on next page Medium Chemical formula Concentration Temp. Product Name Citric acid anhydrous Cat No. 58 / Monday, March 26, 2012 / Rules and Regulations 07/14/2020 EN (English US) 2/6 : Full text of hazard classes and H Publication date 1995 Usage CC0 1.0 Universal Topics data.gov.in, standardsbis.in, public.resource.org . Many specifications include the use of sodium dichromate in the passivation solution, or as a post passivation rinse, to aid in the formation of a chromic oxide film. The citric acid in anhydrous form crystallizes from hot water and is a natural preservative used to add sour taste to food and drink. If not Eur., BP, USP, E330, anhydrous, 99.5-100.5% (based on anhydrous substance) 1.37002 Citric acid, anhydrous powder, EMPROVE EXPERT, Ph. - cube in box INGREDIENTS: LARD, BHA, PROPYL GALLATE AND CITRIC ACID ADDED TO PROTECT FLAVOR. Citric Acid, Anhydrous (Main constituent) (CAS-No.) . There is evidence from published studies that citric acid is safe for the target species when . Hydrochloric acid is the least expensive and most widely uaed solvent for waterside deposits on steels. Implementing a citric acid-based passivation procedure would improve the health and environmental safety aspects of passivation process. Appearance: White crystalline powders, colorless crystals or granules. The information contained herein is correct as of the date of this document to the best of our knowledge. Citric acid CAS 77-92-9 anhydrous powder EMPROVE ESSENTIAL Ph Eur,BP,ChP,JP,USP,E 330,FCC - Find MSDS or SDS, a COA, data sheets and more information. Avoid contact with skin, eyes and clothing. Details of the supplier of the safety data sheet 2. . Vitamin B. Information on basic physical and chemical properties Appearance Crystals or crystalline Colour White. Eyes . It can occur in two forms - monohydrate or water-free (anhydrous). It is an important metabolite in the pathway of all aerobic organisms. CitriSurf 2250 is the citric acid solution most commonly used by our customers. The Anhydrous Citric Acid monograph will be incorporated into and become official with Supplement 1 to USP 35-NF 30. It is based on using an acid (nitric or citric) under highly controlled conditions to remove free iron particles from the surface and to help form a metal oxide layer that increases its . NFPA - 50% Citric Acid Solution Blue (Health) : 2 Red (Fire) : 0 Yellow (Reactivity) : 0 White (Special) : _ AQUAPLJLSE a FLYNN ROAD CAMARILLO, CA 93012 PHONE: Skin contact H. 8. SYNONYMS INS No. Citric acid is a tribasic acid, with pK a values, extrapolated to zero ionic strength, of 3.128, 4.761, and 6.396 at 25 C. PRODUCT SPECIFICATION SHEET Citric Acid USP Grade Test Specification Typical Result Assay 99.5 - 100.5% 99.92% Transmittance 96.0 99.4 Identification To Pass Test Pass Color & Clarity of Solution To Pass Test Pass Water 0.5% 0.15% Heavy Metals 5 ppm 1 ppm Oxalate 100 ppm 30 ppm Sulphate 150 ppm 10 ppm Calcium 75 ppm 4 ppm PDF Specification Document: Enter Lot Number Go: 1002419029: Double PE Sack: PDF Specification Document: Enter Lot Number Go: Certificates. 10.3 Possibility of hazardous reactions No dangerous reactions known. With the help of quality assured raw materials and modern technology, we are manufacturing quality high gamut of Citric Acid - Anhydrous. Name Type 20110001362.pdf STI cloud_download content_copy visibility . 4.1 Description of first aid measures . Usually, these tablets are prepared by compressing the active ingredients with mixture of sodium bicarbonate and organic acids such as citric and tartaric acid. Citric acid is an ingredient of citrated anticoagulant solutions; and also a reactive intermediate in chemical synthesis. SINGLE PAGE PROCESSED JP2 ZIP download. It is considered as a tribasic acid. IS 5464: Citric acid, monohydrate by Bureau of Indian Standards. ASTM A967 citric acid passivation treatments. 150 years Environmental comparison Organic acids Inorganic acids Formic acid Citric acid Acetic acid Lactic acid Nitric acid Phosphoric acid Sulfuric acid Sulfamic acid Chemical Oxygen Demand g O 2 / kg acid 348 750 1067 1067 N/A N/A N/A N/A Categories. 03-201807 Citric Acid Anhydrous Page 3/3 3 Chloride Not more than 50ppm Mesh size 8-80mesh We're Citric Acid Monohydrate Manufacturers, Suppliers and Wholesalers in China. temperature and 160F. download 1 file . 2A, H319 . 7. E-Number (E-NR): E330 EINECS: 20-10-691 Ingredient: Citric acid Storage / Shelf-life Citric Acid Anhydrous is slightly hydroscopic and should be stored under conditions of low temperature and low humidity in Citric Acid Specification Sheet Identifier CAS Number : 77 - 92 - 9 Properties Molecular Formula : C6H8O7 Molecular Mass : 192.12 g/mol . 1 Generally, these tablets are included drugs that are solved rapidly when entered to water and they are recommended as a . Product Specification FRUIT ACID /BOX / 4X 1KG_EN 2.01501.112 22.11.2016 - Version of specification: 1.1 - 05 Fi EN St - page 1 von 5 , , , 1. SENSORY Taste: sour Odor: typical **Should you have any questions about the Anhydrous Citric Acid monograph, please contact Dr. Tong (Jenny) Liu (240-221-2072 or jyl@usp.org ). Citric acid and trisodium citrate are widely used additives in the food and beverages industry where they are greatly desired for their pleasant taste, pH properties and excellent solubility. However although there is a lack of published studies that conclusively prove citric acid is a technically sound passivation agent. Folic Acid (mcg) 0 0 0 0 0 . Group ADI "Not limited" for citric acid and its calcium, potassium, sodium and ammonium salts established at the 17th JECFA in 1973. Citric acid is a tricarboxylic acid that is propane-1,2,3-tricarboxylic acid bearing a hydroxy substituent at position 2. Ecological information 12.1 Toxicity Toxicity to fish Citric acid anhydrous LC50: 440 mg/l Exposure time: 48 h Species: Leuciscus idus (Golden Ode) static test Method: OECD Test Guideline 203 Toxicity to daphnia and other aquatic invertebrates. The combination of citric acid solutions available to test was too large to handle so a 3 factor - 2 level Design of Experiment5 (DoE) was conducted to determine the optimum Citric Acid 49-51 77-92-2 201-069-1 C. 6. . Passivation is a process of making stainless steel more stainless than it would be if left alone. CAMEO Chemicals. Alcohol (g) 0 0 0 0 0 . General industries use this standard to describe and control the passivation of stainless steel. Essentially circular Sugar molasses, the sidestreams from sugar refineries, make up the primary raw material for our unique natural production process. and FeaO*. Citric acid anhydrous Toxicity to algae Citric acid anhydrous H2O Formula weight, monohydrate 210.14 INS: 330 CAS: anhydrous [CAS 77-92-9] CAS: monohydrate [CAS 5949-29-1] DESCRIPTION Citric Acid occurs as colorless, translucent crystals or as a white, granular to fine, crystalline powder. ASTM A 967-05 SPECIFICATIONS Nitric Acid Methods Nitric 1: 20-25 v% Nitric Acid, 2.5 w% Sodium Dichromate, 120-130F, 20 minutes minimum . Solution Composition (wt %) acetic, phosphoric, and citric acid, or caustic soda. [1] The first citric acid fermentations were carried out in surface cultures. Citric Acid is a weak acid with a chemical formula C 6 H 8 O 7. Citric acid based formulations are evolved for nuclear structural materials to avoid chloride contamination. this analytical method is a validated measurement procedure for the determination of citric acid [77-92-9] in workplace air in a concentration range of one tenth up to twice the currently valid. [NOTEThe Sample solution is to be compared to Stan-Sample solution: Prepare as directed in the test for dard suspension A in diffused daylight 5 min after prep-Clarity of Solution. ASTM A967. Citric acid anhydrous 12.4 Mobility in soil The product is miscible in water and readily biodegradable in both water and soil. TEXT . Package 25kg net 3-ply kraft paper bags or composite paper-plastic bags, 500kg or 1000kg net PP woven Nitric acid concentrations in the 20% to 50% by volume range are generally specified. After inhalation: In case of unconsciousness place patient stably in side position for transportation. we still see specifications for the "same old same old" circa 1975. We will be investigating four such fruit juices . Table 2 Metal Content Of Citric Acid Bath After 30 Days Passivation Of 316L SS Citric Acid Titration Metals in Citric Acid Solution (mg/L) Fe Ni Cr Cd Mn Before Passivation 4.44% <0.05 <0.05 <0.05 <0.02 <0.05 After Passivation 4.40% 0.72 <0.05 <0.05 <0.02 <0.05 Each company using citric acid passivation is responsible for making sure Tate & Lyle Citric Acid - Fine Specification Sheet Page 2 of 6 Version 1.12 (Date of Last Change:23-Apr-18) Date Printed: 17-Dec-18 THRU US#100 (150m) <= 5.00 % Particle Size - Gradex TN20745G Product Composition / Labeling Citric Acid Regulatory Status Compliance Statement: Complies with FDA Regulation 21CFR.184.1033 PDF Specification Document: Enter Lot Number Go: 8187075000: Plastic bottle: PDF Specification Document: Enter Lot Number Go: Related Products & Applications. Group ADI "Not limited" for citric acid and its calcium, potassium, sodium and ammonium salts established at the 17th JECFA in 1973. No. and does not replace any product information or product specification. Eye contact Rinse thoroughly with plenty of water for at least 15 minutes, lifting lower and upper eyelids. CITRIC ACID SECTION 9: PHYSICAL AND CHEMICAL PROPERTIES 9.1. Citric acid anhydrous 12. Citric acid (anhydrous and monohydrate) is already authorised for use in food following the quantum satis principle. 120 Odour Odourless. Cargill Citric Acid is manufactured to meet the monograph her for melts at 153C (307F). . 17 Technical Data Corrosion resistance table Citric acid (continued) C 3 H 4 Solubility Soluble in water. The most important finding was that Aspergillus niger grew well at pH values around 2.5-3.5 and high concentrations of sugars favour citric acid production. 4. The regulation requires that the citric acid produced conforms to the specifications of the 119 Food Chemicals Codex (Food Chemicals Codex, 2010). History In the 1930s, some units were implanted It is also used as antioxidant, plasticizer and detergent in chemical, cosmetics and cleaning industries. 77-92-9 100 Eye Irrit. The formulations can be based on strong acid or weak acid and optimisation is necessary far an effective composition. 330 Resists distortion and retains strength up to 135C (275F). FIRST-AID MEASURES Description of first aid measures Inhalation Remove to fresh air. An application has been made for the authorisation of citric acid (anhydrous and monohydrate) when used as an acidity regulator in feed and in water for drinking for all animal species. Ideal to handle wet and dry chlorine, bromine, and other halogen services. Glycolic acid is paired with hydrochloric acid in one popular blend. Flush with clean water. On the pH scale, citric acid is a weaker acid with a pH ranging between 3 and 6. In 1784, a Swedish chemist named Carl Wilhelm Scheele first extracted citric acid from lemon juice by fermenting molasses or cane sugar with the help of a fungus ( Aspergillus niger ). Citric acid comes as a white fine grain powder. 441.3 Citric Acid 441.3.1 If citric acid is used as a color stabilizer, the amount that can be used may be based on the amount needed to adjust the pH of the liquid whole eggs to a pH of 6.5-6.8 rather than the maximum of 0.2 percent permitted. If breathing is difficult, give oxygen. It is odourless, sour in taste, and appears as a white crystalline solid. 25 KGS. Citric Acid Anhydrous Molecular Formula C 6 H 8 O 7 Molecular Weight 192.13 77 -92 9 E-NR E 330 EINECS 20-10-691 Product Specifications Assay (%) 99.5 - 100.5 Water (%) 0.5 max Identification Passes USP/FCC tests Residue on Ignition (%) 0.05 max CITRIC ACID Prepared at the 53rd JECFA (1999) and published in FNP 52 Add 7 (1999), superseding specifications prepared at the 51st JECFA (1998), published in FNP 52 Add 6 (1998). SECTION 4: FIRST AID MEASURES . [20] The pK a of the hydroxyl group has been found, by means of 13 C NMR spectroscopy, to be 14.4. Citric Acid, the European Pharmacopoeia (9.0) monograph for Citric Acid, Anhydrous and the FAO JECFA (2006) monograph for Citric Acid. 4. Effervescent tablets were designed to produce solutions that release carbon dioxide simultaneously. Page 1 o f 7 MSDS - Citric Acid Material Safety Data Sheet (MSDS) - Citric acid 1.Chemical Product and Company Identification Product Name : Citric acid Catalog Codes : SLC5449, SLC2665, SLC4453, SLC1660,SLC3451 CAS# : 77 -92 -9 RTECS : GE7350000 TSCA : TSCA 8(b) inventory: Citric acid The citric acid cycle is a series of chemical reactions of central importance in all living cells that utilize oxygen to generate useful energy by cellular respiration. Move casualty to fresh air and keep at rest. 5949-29-1 Citric acid monohydrate Oral NOAEL 1200mg/kg/day mg/kg (No information available) Repeat dose toxicity Irritation of skin Skin corrosion/Irritation mild irritant (rabbit) (OECD 405, 72h) . The standard also allows any combination of citric acid concentration, temperature and time, provided that the passivation test criteria can be met. Hazard(s . C 304 cr 18 ni 9 cr 17 316 ni 12 mo 2,5. Uses advised against Food, drug, pesticide or biocidal product use. Product description. Please note, the CitriSurf offers top passivation performance to prevent corrosion of stainless steel parts. Wash hands before breaks and at Directive 89/686/EEC and EN 374 Respiratory protection. Consult a physician. Most blends include surfactant and dispersant . 1 Oxalic acid 1.23 1.12 19471 64904 2 cis-Aconitic acid 1.29 1.15 16122 53741 3 Tartaric acid 1.30 1.24 19272 64240 4 Malic acid 1.10 1.07 20153 67176 5 Lactic acid 1.16 1.10 21469 71563 6 Formic acid 1.08 1.05 22118 73726 7 Fumaric acid 1.05 1.03 15751 52504 8 Propionic acid 1.12 1.09 20492 68305 9 Butyric acid 1.15 1.13 18181 60603 2 1 3 4 5 . PRODUCT CHARACTERISTICS: REFINED LARD THAT IS MANUFACTURED UNDER USDA SUPERVISION. Citric acid is the common weak organic acid derived from the Latin word " Citrus ". 330 DEFINITION Citric acid may be produced by recovery from sources such as lemon or The genus (Citrus) includes all the species of Lemon, orange etc. O.
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